简介概要

In situ synchrotron X-ray diffraction analysis of deformation behavior of a Nb/NiTi composite for biomedical applications

来源期刊:Rare Metals2021年第3期

论文作者:Shun Guo Rui-Tang Wu Yu-Lu Shi Yan-Pin Hou Wen Ma Guang-Lei Liu Hai-Xia Liu Xiao-Nong Cheng

文章页码:600 - 606

摘    要:The deformation behavior involved in Nb/NiTi composite for biomedical applications within a large macroscopic strain range was investigated by tensile loading-unloading test and in situ synchrotron X-ray diffraction(SXRD).Experimental results show that during loading,the Nb/NiTi composite experiences the elastic elongation of B2-NiTi austenitic,B19’-NiTi martensitic and β-Nb phases,B2→ B19’ stress-induced martensitic(SIM) transformation and tensile plastic deformation of β-Nb phase.During unloading,the deformation behavior involved in Nb/NiTi composite includes the elastic recovery of B2-NiTi austenitic,B19’-NiTi martensitic and β-Nb phases,reverse phase transformation B19’→B2 and compressive deformation of p-Nb phase.The martensitic transformation in this composite is almost reversible and occurs in a localized manner.These results might contribute to a comprehensive understanding of the deformation mechanism involved in Nb/NiTi composite and shed some light on design and development of novel composites with a combination of good biocompatibility and excellent superelasticity for biomedical applications.

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In situ synchrotron X-ray diffraction analysis of deformation behavior of a Nb/NiTi composite for biomedical applications

Shun Guo1,Rui-Tang Wu1,Yu-Lu Shi1,Yan-Pin Hou1,Wen Ma1,2,Guang-Lei Liu1,Hai-Xia Liu1,Xiao-Nong Cheng1

1. School of Materials Science and Engineering,Jiangsu University

摘 要:The deformation behavior involved in Nb/NiTi composite for biomedical applications within a large macroscopic strain range was investigated by tensile loading-unloading test and in situ synchrotron X-ray diffraction(SXRD).Experimental results show that during loading,the Nb/NiTi composite experiences the elastic elongation of B2-NiTi austenitic,B19’-NiTi martensitic and β-Nb phases,B2→ B19’ stress-induced martensitic(SIM) transformation and tensile plastic deformation of β-Nb phase.During unloading,the deformation behavior involved in Nb/NiTi composite includes the elastic recovery of B2-NiTi austenitic,B19’-NiTi martensitic and β-Nb phases,reverse phase transformation B19’→B2 and compressive deformation of p-Nb phase.The martensitic transformation in this composite is almost reversible and occurs in a localized manner.These results might contribute to a comprehensive understanding of the deformation mechanism involved in Nb/NiTi composite and shed some light on design and development of novel composites with a combination of good biocompatibility and excellent superelasticity for biomedical applications.

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