Hydrothermal Synthesis of WO3 Nanowires in the Presence of Guanidine Sulfate and Its Photocatalytic Activity
来源期刊：Journal Of Wuhan University Of Technology Materials Science Edition2016年第4期
论文作者：牟婉君 YU Qianhong LI Xingliang WEI Hongyuan 蹇源
文章页码：731 - 735
摘 要：WO3 nanowires were fabricated by a hydrothermal method,which proceeded at 170 ℃ for 48 h in a solution containing C2H10N6H2SO4 as a dispersant and Na2WO4 as a starting material.The nanowires exhibit a well crystallized one-dimensional structure with 20 nm in diameter and several microns in length.The physicochemical properties of WO3 were compared using X-ray diffraction（XRD）,scanning electron microscopy（SEM）,transmission electron microscopy（TEM）,energy dispersive X-ray spectroscopy（EDX） and UV-vis spectroscopy（UV-Vis）.The photoactivity of the as-perpared WO3 nanowires was evaluated through the photodegradation of methylene blue（MB） in aqueous solution.The experimental results demonstrate that addition of C2H10N6H2SO4 salt in the WO3 nanowires synthesis process can enhance its photocatalytic activity obviously.
牟婉君，YU Qianhong，LI Xingliang，WEI Hongyuan，蹇源
Institute of Nuclear Physics and Chemistry,China Academy of Engineering Physics
摘 要：WO3 nanowires were fabricated by a hydrothermal method,which proceeded at 170 ℃ for 48 h in a solution containing C2H10N6H2SO4 as a dispersant and Na2WO4 as a starting material.The nanowires exhibit a well crystallized one-dimensional structure with 20 nm in diameter and several microns in length.The physicochemical properties of WO3 were compared using X-ray diffraction（XRD）,scanning electron microscopy（SEM）,transmission electron microscopy（TEM）,energy dispersive X-ray spectroscopy（EDX） and UV-vis spectroscopy（UV-Vis）.The photoactivity of the as-perpared WO3 nanowires was evaluated through the photodegradation of methylene blue（MB） in aqueous solution.The experimental results demonstrate that addition of C2H10N6H2SO4 salt in the WO3 nanowires synthesis process can enhance its photocatalytic activity obviously.
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