Preparation and characterization of jet-electrodeposited nanocrystalline nickel coatings

来源期刊：中国有色金属学报(英文版)2007年增刊第1期(Part ⅡB)

论文作者：潘勇 江山 戴翠英 唐甜 周兆锋 周益春

文章页码：770 - 775

Key words：nanocrystalline nickel; jet-electro deposition; deposition current density; jet velocity

Abstract: Nanocrystalline nickel coatings were prepared by both direct current(DC) and pulse current(PC) jet-electrodeposition. The influences of current density and jet velocity on the surface morphology, microstructure and preferred orientation of the coatings obtained were investigated by SEM, TEM and XRD. It is found that the current density strongly affects the microstructure of the nickel coating. An increase of the DC current density results in a slight increase of the grain size and preferred orientation progressive evolution (i.e. from (111) to (200)), whereas an increase of the PC current density leads to a certain decrease of the grain size and preferred orientation change (i.e. from (111) to a strong (220)). Moreover, jet velocity shows no significant effect on the grain size and preferred orientation for the nanocrystalline coatings obtained in both DC and PC within the range of jet velocity studied.

基金信息：the Hi-tech Research and Development Program of China
Fund for Prominent Young Scholars from the Organization of NNSF of China
Scientific Research Fund of Hunan Provincial Education Department, China