Effect of cobalt substitution on magnetic properties and microstructure of nanocrystalline(NdDyTb)12.3(FeZrNbCu)81.7B6.0 ribbons
来源期刊:Journal of Rare Earths2009年第3期
论文作者:包小倩 高学绪 张茂才 朱洁 周寿增
文章页码:501 - 505
摘 要:Effect of Co substitution and annealing treatment on the formation,magnetic properties and microstructure of(NdDyTb) 12.3(FeZrNbCu) 81.7-xCoxB6(x=0-15) ribbons prepared by rapid quenching and subsequent annealing was systematically investigated by means of differential scanning calorimeter(DSC) ,X-ray diffraction(XRD) ,high resolution scanning electron microscopy(HRSEM) and vibrating sample magnetometer(VSM) . Phase analysis revealed single-phase material. The remanence polarization Jr and maximum energy product(BH) max increased with increasing x from 0 to 12 and then decreased for x=15. The intrinsic coercivity Hci of(NdDyTb) 12.3(FeZrNbCu) 81.7-xCoxB6 ribbons optimally processed decreased from 1308.7 kA/m for x=0 to 817.4 kA/m for x=15. Optimum magnetic properties with Jr=1.041 T,Hci=944.9 kA/m and(BH) max=155.1 kJ/m3 were achieved by annealing melt-spun ribbon(x=12) at 675 °C for 10 min. There was no significant influence of Co substitution on microstructure.
包小倩,高学绪,张茂才,朱洁,周寿增
摘 要:Effect of Co substitution and annealing treatment on the formation,magnetic properties and microstructure of(NdDyTb) 12.3(FeZrNbCu) 81.7-xCoxB6(x=0-15) ribbons prepared by rapid quenching and subsequent annealing was systematically investigated by means of differential scanning calorimeter(DSC) ,X-ray diffraction(XRD) ,high resolution scanning electron microscopy(HRSEM) and vibrating sample magnetometer(VSM) . Phase analysis revealed single-phase material. The remanence polarization Jr and maximum energy product(BH) max increased with increasing x from 0 to 12 and then decreased for x=15. The intrinsic coercivity Hci of(NdDyTb) 12.3(FeZrNbCu) 81.7-xCoxB6 ribbons optimally processed decreased from 1308.7 kA/m for x=0 to 817.4 kA/m for x=15. Optimum magnetic properties with Jr=1.041 T,Hci=944.9 kA/m and(BH) max=155.1 kJ/m3 were achieved by annealing melt-spun ribbon(x=12) at 675 °C for 10 min. There was no significant influence of Co substitution on microstructure.
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