Hydro(Solvo) Thermal Synthesis and Characterization of Bax Sr1-x TiO3 Nanopowders
来源期刊:材料保护2004年增刊第2期
论文作者:YANG Zhi-min YANG Jian DU Jun MAO Chang-hui XING Guang-jian
关键词:nanopowder; characterization; hydorthermal methods; solvothermal methods;
摘 要:Nano-sized barium strontium titanate (BaxSr1-x TiO3, BST) powders were synthesized with hydrothermal and solvothermal methods at 120 ℃ for 4 h based on the reaction precursor of barium acetate, strontium acetate, tetrabutyl titanium and (CH3 )4NOH. The crystalline phase, particle size and morphology of the BST powders were characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM). Influences of reaction temperature and reaction time on the morphologies of powders were also discussed.
YANG Zhi-min1,YANG Jian1,DU Jun1,MAO Chang-hui1,XING Guang-jian1
(1.General Research Institute for Nonferrous Metals, Beijing 100022, P.R. China)
摘要:Nano-sized barium strontium titanate (BaxSr1-x TiO3, BST) powders were synthesized with hydrothermal and solvothermal methods at 120 ℃ for 4 h based on the reaction precursor of barium acetate, strontium acetate, tetrabutyl titanium and (CH3 )4NOH. The crystalline phase, particle size and morphology of the BST powders were characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM). Influences of reaction temperature and reaction time on the morphologies of powders were also discussed.
关键词:nanopowder; characterization; hydorthermal methods; solvothermal methods;
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