Microstructure and Property of AlN Joint Brazed with Au–Pd–Co–Ni–V Brazing Filler
来源期刊：JOURNAL OF MATERIALS SCIENCE TECHNOLOG2015年第10期
论文作者：Bo Chen Huaping Xiong Yaoyong Cheng Wei Mao Shibiao Wu
文章页码：1034 - 1038
摘 要：An Au–Pd–Co–Ni–V brazing alloy was designed for Al N ceramic joining. Its wettability on Al N was studied with the sessile drop method. The results showed that the contact angle was decreased gradually with increasing temperature and the prolonging of holding time. Sound Al N/Al N joints were achieved with the brazing alloy at 1170 °C for 10 min. The microstructure of the Al N/Al N joints was examined by scanning electron microscopy（SEM）. It was found that element V played the active role in the interfacial reaction between the ceramic and the brazing alloy. V reacted with N decomposed from Al N, resulted in the formation of V–N compound. Based on the energy-dispersive spectroscopy（EDS）and X-ray diffraction（XRD） analysis results, the V–N reaction product was verified as V2 N. The overall reaction during the brazing process can be described by the following equation: 2V + AlN + 2Pd = V2 N + Pd2 Al.The Al N/Al N joints brazed with the Au–Pd–Co–Ni–V brazing alloy exhibited three-point bend strength of 162.7 MPa at room temperature, and under the bend test the fracture of the joint occurred at the Al N ceramic substrate.
Bo Chen，Huaping Xiong，Yaoyong Cheng，Wei Mao，Shibiao Wu
Welding and Plastic Forming Division,Beijing Institute of Aeronautical Materials
摘 要：An Au–Pd–Co–Ni–V brazing alloy was designed for Al N ceramic joining. Its wettability on Al N was studied with the sessile drop method. The results showed that the contact angle was decreased gradually with increasing temperature and the prolonging of holding time. Sound Al N/Al N joints were achieved with the brazing alloy at 1170 °C for 10 min. The microstructure of the Al N/Al N joints was examined by scanning electron microscopy（SEM）. It was found that element V played the active role in the interfacial reaction between the ceramic and the brazing alloy. V reacted with N decomposed from Al N, resulted in the formation of V–N compound. Based on the energy-dispersive spectroscopy（EDS）and X-ray diffraction（XRD） analysis results, the V–N reaction product was verified as V2 N. The overall reaction during the brazing process can be described by the following equation: 2V + AlN + 2Pd = V2 N + Pd2 Al.The Al N/Al N joints brazed with the Au–Pd–Co–Ni–V brazing alloy exhibited three-point bend strength of 162.7 MPa at room temperature, and under the bend test the fracture of the joint occurred at the Al N ceramic substrate.
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