Separation of baicalin from Scutellaria Baicalensis Georgi with polyamide
来源期刊:中南大学学报(英文版)2008年第5期
论文作者:池汝安 周芳 黄琨 张越非
文章页码:606 - 606
Key words:baicalin; Scutellaria Baicalensis Georgi; adsorption; separation
Abstract: Separation of baicalin from Scutellaria Baicalensis Georgi with polyamide was studied. The adsorption isotherm, kinetic equation and desorption law were investigated by static and dynamic adsorption methods. The results show that the kinetic behavior is mainly controlled by the liquid film diffusion process and obeys the Boyd film diffusion equation. Equilibrium data for the adsorption of baicalin are correlated with Freundlich isotherm equation, i.e. q=3.8ce2.057, suggesting that the relative capacity of polyamide to baicalin is somewhat small. The desorption results indicate that the baicalin with mass fraction of 33.86% and the least impurities can be obtained by chromatography using 60% ethanol as the eluant at room temperature.
基金信息:the Natural Science Foundation of Hubei Province, China