块体纳米晶Al-Zn-Mg-Cu合金的热处理
来源期刊:中国有色金属学报2007年第1期
论文作者:陈汉宾 程军胜 杨滨 张济山 樊建中 田晓风
文章页码:30 - 30
关键词:铝合金;块体纳米晶;低温球磨;固溶处理;时效处理;微观组织
Key words:aluminum alloy; bulk nanocrystalline; cryomilling; solid-solution; aging; microstructure
摘 要:利用液氮球磨、真空热压和挤压工艺制备块体纳米晶Al-Zn-Mg-Cu合金,并对其固溶和时效处理进行研究,得到时效硬度曲线。利用X射线衍射仪和透射电镜对该合金热处理前后的微观组织进行分析,结果表明:块体制备过程中析出的MgZn2可以通过固溶处理使其回溶并在时效后沉淀析出;热压后晶粒尺寸为50~100 nm,热处理后晶粒长大到100 nm,部分晶粒达到200 nm。
Abstract: Bulk nanocrystalline Al-Zn-Mg-Cu alloy was fabricated by cryomilling combined with vacuum hot pressing and extrusion. The aging-curve was obtained. The crystal structures and microstructures before and after heat treatment were investigated by X-ray diffractometry (XRD) and transmission electron microscopy(TEM), respectively. The results show that the deposition(MgZn2) of consolidation can be dissolved again by solid-solution, and precipitated during aging. The grain sizes of the bulk nanocrystalline Al-Zn-Mg-Cu alloy produced by vacuum hot pressing are 50-100 nm, some of them grow to 100 nm even part of them reach 200 nm after heat-treatment.
基金信息:国家高技术研究发展计划资助项目